We irradiate 3 times for 1 minute with 30 second breaks between sessions Otherwise, the reaction will be carried out incorrectly. We wait until the mixture cools down to room temperature
Pour 300 ml of water, possibly with ice, into the mixture and mix thoroughly. An insoluble cuo suspension and iodine are observed in rm, which should uniformly fill all reaction volume by stirring I partially dissolve the precursor with stirring and add aq
